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首頁日本水質法規定的農藥標準品

63種農藥混標溶液 WQ-4

63種農藥混標溶液
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產品簡介

63種農藥混標溶液 WQ-4(每種20μg/ml乙腈溶液)wako#168-26011,用于農藥殘留分析。

產品詳情

63種農藥混標溶液 WQ-4(每種20μg/ml乙腈溶液)

63種農藥混標溶液 WQ-4(每種20μg/ml乙腈溶液)wako#168-26011,用于農藥殘留分析。
生產廠商:富士-和光化學純藥株式會社
儲存條件:-20°C
GHS: Danger
外觀:淡黃色澄清液體。
Oxamyl, Nitenpyram, Pymetrozine, Monocrotophos, Imidacloprid, Cinosulfuron, Acetamiprid, Thiacloprid, Pyrazosulfuron-ethyl, Cyanazine, Ethoxysulfuron, Fluazifop, (E)-Metominostrobin, Linuron, Acibenzolar-S-methyl, Ametryn, Boscalid, Cumyluron, Benzobicyclon, Prometryn, Diclomezine, Chromafenozide, Simeconazole, Tetraconazole, Naproanilide, Tebuconazole, Pirimiphos-methyl, Triflumizole, Benzofenap, Quizalofop-ethyl, Dinotefuran, Thiamethoxam, Clothianidin, Trinexapac-ethyl, Metribuzin, Bromacil, Bendiocarb, Furametpyr, Cyproconazole, Indanofan, Diflubenzuron, Tetrachlorvinphos (CVMP), Cyprodinil, Fentrazamide, Etobenzanid, Oxadiargyl, Phoxim, Pyrazolynate (Pyrazolate), Difenoconazole, Oxaziclomefone, Pentoxazone, Clomeprop, Silafluofen, MCPA (MCP), Dichlorprop, Propanil (DCPA), Inabenfide, Tiadinil, Thifluzamide, Flusulfamide, Tebufenozide,Fluazinam : 每種19.4 - 20.6ug/ml
(Z)-Pyriminobac-methyl, (E)-Pyriminobac-methyl : 每種 9.7 - 10.3ug/ml

分析案例

液相質譜圖譜
63種農藥混標溶液 WQ-4液相質譜圖譜
峰編號 組分 監測離子
(m/z)
模式
前體 產品
1 Oxamyl 237 72 +
2 Pymetrozine 218 105 +
3 Thiamethoxam 292 211 +
4 Trinexapac-ethyl 253 69 +
5 Cinosulfuron 414 183 +
6 Acetamiprid 223 126 +
7 Thiacloprid 253 126 +
8 Pyrazosulfuron-ethyl 415 182 +
9 Cyanazine 241 214 +
10 Bromacil 261 205 +
11 Bendiocarb 224 167 +
12 Ethoxysulfuron 399 261 +
13 Furametpyr 334 157 +
14 (E)-Metominostrobin 285 196 +
15 (Z)-Pyriminobac-methyl*** 362 330 +
16 Ametryn 228 186 +
17 (E)-Pyriminobac-methyl*** 362 330 +
18 Cumyluron 303 185 +
19 Cyproconazole 292 70 +
20 Prometryn 242 158 +
21 Chromafenozide 395 175 +
22 Simeconazole 294 70 +
23 Naproanilide 292 171 +
24 Tebufenozide 351 133 +
25 Difenoconazole 406 251 +
26 Triflumizole 346 278 +
27 Benzofenap 431 105 +
28 Quizalofop-ethyl 373 299 +
29 Oxaziclomefone 376 190 +
30 Dinotefuran 203 129 +
31 Nitenpyram 271 56 +
32 Monocrotophos 224 193 +
33 Imidacloprid 256 209 +
34 Clothianidin 250 132 +
35 Metribuzin 215 49 +
36 Fluazifop 328 282 +
37 Linuron 249 182 +
38 Acibenzolar-S-methyl 211 136 +
39 Boscalid 343 307 +
40 Benzobicyclon 447 257 +
41 Diclomezine 255 141 +
42 Tetraconazole 372 159 +
43 Indanofan 341 175 +
44 Diflubenzuron 311 158 +
45 Tetrachlorvinphos
(CVMP)
367 127 +
46 Tebuconazole 308 70 +
47 Cyprodinil 226 108 +
48 Fentrazamide 350 154 +
49 Etobenzanid 340 179 +
50 Oxadiargyl 358 341 +
51 Phoxim 299 77 +
52 Pirimiphos-methyl 306 164 +
53 Pyrazolate 439 91 +
54 Clomeprop 324 120 +
55 Pentoxazone 371 286 +
56 Silafluofen 426 287 +
57 MCPA(MCP) 199 141 -
58 Dichlorprop 233 161 -
59 Propanil(DCPA) 216 160 -
60 Inabenfide 337 122 -
61 Tiadinil 266 71 -
62 Thifluzamide 527 125 -
63 Flusulfamide 413 171 -
64 Fluazinam 463 416 -
* 該產品含2%甲醇。
** 分析條件,圖標和檢測離子僅供參考。不能當作農藥混合標準溶液的確定數據使用。
*** 制備溶液濃度,作為E和Z型異構體的總和,可轉換成20 µg/mL(每種10 μg/mL)。
檢測條件
【儀器】
島津 LCMS-8040
【液相條件】
柱子:Wakopak? Ultra C18-3 2.0 × 75 mm
柱溫:40 ℃
洗脫液:A) 5 mmol/L甲酸銨水溶液;B) 5 mmol/L甲酸銨甲醇溶液
梯度
時間 (分鐘) B 濃度(%)
0-2 5
2-6 5-40
6-41 40-75
41-45 75-100
46-50 100
50-50.01 100-5
50.01-60 5
流速:0.15 毫升/分鐘
【質譜條件】
電離:ESI(電噴霧電離)
模式:多反應檢測掃描(MRM)

產品列表

產品編號 產品名稱 產品級別 包裝
164-26013 63 Pesticides Mixture Standard Solution WQ-4 (each 20μg/ml Acetonitrile Solution)
63種農藥混標溶液 WQ-4(每種20μg/ml乙腈溶液)
農藥殘留分析 1mLx5A
168-26011 1mL

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