63種農(nóng)藥混標溶液 WQ-4（每種20μg/ml乙腈溶液）wako#168-26011，用于農(nóng)藥殘留分析。

生產(chǎn)廠商：富士-和光化學(xué)純藥株式會社
儲存條件：-20°C
GHS: Danger
外觀：淡黃色澄清液體。

Oxamyl, Nitenpyram, Pymetrozine, Monocrotophos, Imidacloprid, Cinosulfuron, Acetamiprid, Thiacloprid, Pyrazosulfuron-ethyl, Cyanazine, Ethoxysulfuron, Fluazifop, (E)-Metominostrobin, Linuron, Acibenzolar-S-methyl, Ametryn, Boscalid, Cumyluron, Benzobicyclon, Prometryn, Diclomezine, Chromafenozide, Simeconazole, Tetraconazole, Naproanilide, Tebuconazole, Pirimiphos-methyl, Triflumizole, Benzofenap, Quizalofop-ethyl, Dinotefuran, Thiamethoxam, Clothianidin, Trinexapac-ethyl, Metribuzin, Bromacil, Bendiocarb, Furametpyr, Cyproconazole, Indanofan, Diflubenzuron, Tetrachlorvinphos (CVMP), Cyprodinil, Fentrazamide, Etobenzanid, Oxadiargyl, Phoxim, Pyrazolynate (Pyrazolate), Difenoconazole, Oxaziclomefone, Pentoxazone, Clomeprop, Silafluofen, MCPA (MCP), Dichlorprop, Propanil (DCPA), Inabenfide, Tiadinil, Thifluzamide, Flusulfamide, Tebufenozide,Fluazinam : 每種19.4 - 20.6ug/ml

(Z)-Pyriminobac-methyl, (E)-Pyriminobac-methyl : 每種 9.7 - 10.3ug/ml

分析案例

液相質(zhì)譜圖譜

峰編號 組分 監(jiān)測離子 (m/z) 模式 峰編號 組分 監(jiān)測離子 (m/z) 模式 峰編號 組分 監(jiān)測離子 (m/z) 模式 前體 產(chǎn)品 前體 產(chǎn)品 前體 產(chǎn)品 1 Oxamyl 237 72 + 22 Simeconazole 294 70 + 43 Indanofan 341 175 + 2 Pymetrozine 218 105 + 23 Naproanilide 292 171 + 44 Diflubenzuron 311 158 + 3 Thiamethoxam 292 211 + 24 Tebufenozide 351 133 + 45 Tetrachlorvinphos (CVMP) 367 127 + 4 Trinexapac-ethyl 253 69 + 25 Difenoconazole 406 251 + 46 Tebuconazole 308 70 + 5 Cinosulfuron 414 183 + 26 Triflumizole 346 278 + 47 Cyprodinil 226 108 + 6 Acetamiprid 223 126 + 27 Benzofenap 431 105 + 48 Fentrazamide 350 154 + 7 Thiacloprid 253 126 + 28 Quizalofop-ethyl 373 299 + 49 Etobenzanid 340 179 + 8 Pyrazosulfuron-ethyl 415 182 + 29 Oxaziclomefone 376 190 + 50 Oxadiargyl 358 341 + 9 Cyanazine 241 214 + 30 Dinotefuran 203 129 + 51 Phoxim 299 77 + 10 Bromacil 261 205 + 31 Nitenpyram 271 56 + 52 Pirimiphos-methyl 306 164 + 11 Bendiocarb 224 167 + 32 Monocrotophos 224 193 + 53 Pyrazolate 439 91 + 12 Ethoxysulfuron 399 261 + 33 Imidacloprid 256 209 + 54 Clomeprop 324 120 + 13 Furametpyr 334 157 + 34 Clothianidin 250 132 + 55 Pentoxazone 371 286 + 14 (E)-Metominostrobin 285 196 + 35 Metribuzin 215 49 + 56 Silafluofen 426 287 + 15 (Z)-Pyriminobac-methyl*** 362 330 + 36 Fluazifop 328 282 + 57 MCPA(MCP) 199 141 - 16 Ametryn 228 186 + 37 Linuron 249 182 + 58 Dichlorprop 233 161 - 17 (E)-Pyriminobac-methyl*** 362 330 + 38 Acibenzolar-S-methyl 211 136 + 59 Propanil(DCPA) 216 160 - 18 Cumyluron 303 185 + 39 Boscalid 343 307 + 60 Inabenfide 337 122 - 19 Cyproconazole 292 70 + 40 Benzobicyclon 447 257 + 61 Tiadinil 266 71 - 20 Prometryn 242 158 + 41 Diclomezine 255 141 + 62 Thifluzamide 527 125 - 21 Chromafenozide 395 175 + 42 Tetraconazole 372 159 + 63 Flusulfamide 413 171 -   64 Fluazinam 463 416 - * 該產(chǎn)品含2%甲醇。 ** 分析條件，圖標和檢測離子僅供參考。不能當(dāng)作農(nóng)藥混合標準溶液的確定數(shù)據(jù)使用。 *** 制備溶液濃度，作為E和Z型異構(gòu)體的總和，可轉(zhuǎn)換成20 μg/mL(每種10 μg/mL)。

檢測條件 【儀器】 島津 LCMS-8040 【液相條件】 柱子：Wakopak? Ultra C18-3　2.0 × 75 mm 柱溫：40 ℃ 洗脫液：A) 5 mmol/L甲酸銨水溶液；B) 5 mmol/L甲酸銨甲醇溶液 梯度 時間 (分鐘) B 濃度(%) 0-2 5 2-6 5-40 6-41 40-75 41-45 75-100 46-50 100 50-50.01 100-5 50.01-60 5 流速：0.15 毫升/分鐘 【質(zhì)譜條件】 電離：ESI（電噴霧電離） 模式：多反應(yīng)檢測掃描（MRM）

產(chǎn)品列表

產(chǎn)品編號	產(chǎn)品名稱	產(chǎn)品級別	包裝
164-26013	63 Pesticides Mixture Standard Solution WQ-4 (each 20μg/ml Acetonitrile Solution) 63種農(nóng)藥混標溶液 WQ-4（每種20μg/ml乙腈溶液）	農(nóng)藥殘留分析	1mLx5A
168-26011			1mL

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